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Also Yan et al. discussed several instances of compound degradation due to hydrolysis and oxidation mechanisms,21 while Darvas et al. demonstrated the stability of a combinatorial library containing a labile core structure with an electro-rich pyrrole moiety could be improved by using electronwithdrawing or bulky substitution.8 Cheng et al. observed several elimination reactions, such as loss of 17 Da (water), 17 Da (ammonia), 36 Da (HCl), and 28 Da (CO).19 In contrast, very few direct oxidation products were observed (e.g., +16, +32 Da) in their study, Table 13.3, and these results correlate well with the observation that the water content in the sample has a more signi cant effect on compound stability than the atmospheric oxygen content. Figure 13.11 gives an example of the degradation products observed for the compounds in this study. Additionally many compounds showed a signi cant decrease in concentration, with no new components identi ed in the UV or MS chromatograms. These results suggest that the observed compound loss was due to precipitation. As the unstable compounds show a broad base-line in the UV chromatogram with no clearly distinguishable new peaks, this is probably due to polymerization. Figure 13.12 shows two examples where compounds were lost with no readily identi ed new UV peaks after storage.Related: The times to execute the path here are 214 and 244 steps, respectively, shorter than in the corresponding examples in Figures 4.12a and 4.12b. The examples thus demonstrate hat better sensing (larger rv ) results in shorter time to complete the task: More crowded space results in longer time, though possibly in shorter paths. Note that in some points the algorithm found it necessary to make use of the stopping path; those points are usually easy to recognize from the sharp turns in the path. For example, in Figure 4.12a the robot came to a halt at points A and D, and in Figure 4.12b it stopped at points A F. 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